results from liquid chromatography with tandem mass spectroscopy (LC-MS/MS) analyses for the toxins (okadaic acid, dinophysis toxin 1, dinophysis toxin 2, azaspiracids 1, azaspiracid 2, azaspiracid 3, as well as total OA equivalents) from shellfish samples collected for lipophilic marine toxin analyses from the coast of Washington and Puget Sound from 2016-02-03 to 2016-12-20
Northwest Fisheries Science Center
Entity
(ENT)
| ID: 54713
| Published / External
Created: 2018-11-08
|
Last Modified: 2022-08-09
Data Set (DS) | ID: 30880
ID: 54713
Entity (ENT)
* Discovery• First Pass
» Metadata Rubric
Item Identification
* » Title | results from liquid chromatography with tandem mass spectroscopy (LC-MS/MS) analyses for the toxins (okadaic acid, dinophysis toxin 1, dinophysis toxin 2, azaspiracids 1, azaspiracid 2, azaspiracid 3, as well as total OA equivalents) from shellfish samples collected for lipophilic marine toxin analyses from the coast of Washington and Puget Sound from 2016-02-03 to 2016-12-20 |
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Short Name | AZA Project Shellfish Data for Lipophilic Toxins In Washington State 2016 |
* Status | Planned |
Creation Date | |
Revision Date | |
• Publication Date | |
* » Abstract |
Site names, coordinates, dates, and times that shellfish samples were collected for lipophilic marine toxin analyses. The results liquid chromatography with tandem mass spectroscopy (LC-MS/MS) analyses for the toxins (okadaic acid, dinophysis toxin 1, dinophysis toxin 2, azaspiracids 1, azaspiracid 2, azaspiracid 3, as well as total OA equivalents) are included. Additionally, the results of a screening assay for lipophilic toxins (PP2A) that detects okadaic acid and the dinophysis toxins are included. |
* Purpose | |
Notes | |
Other Citation Details | |
• Supplemental Information | |
DOI (Digital Object Identifier) | |
DOI Registration Authority | |
DOI Issue Date |
Keywords
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* Spatial Keywords
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Stratum Keywords
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Physical Location
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• » City | |
• » State/Province | |
• Country | |
• » Location Description |
Entity Information
Entity Type | Spreadsheet |
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Active Version? | Y |
Alias | |
Schema Name | PARR |
» Description |
Site names, coordinates, dates, and times that shellfish samples were collected for lipophilic marine toxin analyses. The results liquid chromatography with tandem mass spectroscopy (LC-MS/MS) analyses for the toxins (okadaic acid, dinophysis toxin 1, dinophysis toxin 2, azaspiracids 1, azaspiracid 2, azaspiracid 3, as well as total OA equivalents) are included. Additionally, the results of a screening assay for lipophilic toxins (PP2A) that detects okadaic acid and the dinophysis toxins are included. |
Change Summary |
Data Attributes
Attribute Summary
Score | Req'd? | PKey? | » Name | Data Storage Type | Description |
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100 | No | No | SITE | TEXT | The name or identification number of a given site at which samples were collected. |
100 | No | No | LATITUDE | NUMBER | The latitude of the sampling site in decmal degrees. Units for values are decimal degrees. |
100 | No | No | LONGITUDE | NUMBER | The longitude of the sampling site in decimal degrees. Units for values are decimal degrees. |
100 | No | No | DATE | DATE | The date (local time) on which as sample was collected. |
100 | No | No | TIME | TIME | The time (local time) on the date in which a sample began to be collected. |
100 | No | No | SAMPLEID | TEXT | The name or identification number of a individual samples collected at specific sites. IDs incorporate a 2 letter site code followed by the eight digit sampling date and a 2 digit code signifying the sample type. |
100 | No | No | OA | TEXT | The concentration of okadaic acid measured in a sample. Units for values are micrograms per 100 grams of tissue. |
100 | No | No | DTX-1 | TEXT | The concentration of dinophysis toxin 1 measured in a sample. Units for values are micrograms per 100 grams of tissue. |
100 | No | No | DTX-2 | TEXT | The concentration of dinophysis toxin 2 measured in a sample. Units for values are micrograms per 100 grams of tissue. |
100 | No | No | AZA-1 | TEXT | The concentration of azaspiracid 1 measured in a sample. Units for values are micrograms per 100 grams of tissue. |
100 | No | No | AZA-2 | TEXT | The concentration of azaspiracid 2 measured in a sample. Units for values are micrograms per 100 grams of tissue. |
100 | No | No | AZA-3 | TEXT | The concentration of azaspiracid 3 measured in a sample. Units for values are micrograms per 100 grams of tissue. |
100 | No | No | Total OA equiv. | TEXT | The sum of Okadaic acid, Dinophysis toxin 1 and Dinophysis toxin 2 for a given sample after equivalency factors have been applied. Units for values are micrograms per 100 grams of tissue. |
100 | No | No | PP2A | TEXT | Result of the protein phosphatase 2A screening assay. Units for values are micrograms per 100 grams of tissue. |
100 | No | No | Shellfish Analysis Notes | TEXT | Notes regarding the analyses of specific shellfish samples. |
Attribute Details
Attribute Name | SITE |
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Seq. Order | 1 |
Data Storage Type | TEXT |
Max Length | |
Min Length | |
Required | No |
Primary Key | No |
Precision | |
Scale | |
Status | Active |
Description |
The name or identification number of a given site at which samples were collected. |
General Data Type | TEXT |
Unit of Measure | |
Case Restriction | |
Display Example | |
Format Mask | |
Null Value | |
Null Value Meaning | |
Allowed Values | As provided |
Default Value | |
Foreign Key Relations | |
Derivation | |
Validation Rules |
Attribute Name | LATITUDE |
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Seq. Order | 2 |
Data Storage Type | NUMBER |
Max Length | |
Min Length | |
Required | No |
Primary Key | No |
Precision | |
Scale | |
Status | Active |
Description |
The latitude of the sampling site in decmal degrees. Units for values are decimal degrees. |
General Data Type | NUMBER |
Unit of Measure | decimal degrees |
Case Restriction | |
Display Example | |
Format Mask | |
Null Value | |
Null Value Meaning | |
Allowed Values | As provided |
Default Value | |
Foreign Key Relations | |
Derivation | |
Validation Rules |
Attribute Name | LONGITUDE |
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Seq. Order | 3 |
Data Storage Type | NUMBER |
Max Length | |
Min Length | |
Required | No |
Primary Key | No |
Precision | |
Scale | |
Status | Active |
Description |
The longitude of the sampling site in decimal degrees. Units for values are decimal degrees. |
General Data Type | NUMBER |
Unit of Measure | decimal degrees |
Case Restriction | |
Display Example | |
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Null Value | |
Null Value Meaning | |
Allowed Values | As provided |
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Validation Rules |
Attribute Name | DATE |
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Seq. Order | 4 |
Data Storage Type | DATE |
Max Length | |
Min Length | |
Required | No |
Primary Key | No |
Precision | |
Scale | |
Status | Active |
Description |
The date (local time) on which as sample was collected. |
General Data Type | DATE |
Unit of Measure | |
Case Restriction | |
Display Example | |
Format Mask | |
Null Value | |
Null Value Meaning | |
Allowed Values | As provided |
Default Value | |
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Derivation | |
Validation Rules |
Attribute Name | TIME |
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Seq. Order | 5 |
Data Storage Type | TIME |
Max Length | |
Min Length | |
Required | No |
Primary Key | No |
Precision | |
Scale | |
Status | Active |
Description |
The time (local time) on the date in which a sample began to be collected. |
General Data Type | TIME |
Unit of Measure | |
Case Restriction | |
Display Example | |
Format Mask | |
Null Value | |
Null Value Meaning | |
Allowed Values | As provided |
Default Value | |
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Derivation | |
Validation Rules |
Attribute Name | SAMPLEID |
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Seq. Order | 6 |
Data Storage Type | TEXT |
Max Length | |
Min Length | |
Required | No |
Primary Key | No |
Precision | |
Scale | |
Status | Active |
Description |
The name or identification number of a individual samples collected at specific sites. IDs incorporate a 2 letter site code followed by the eight digit sampling date and a 2 digit code signifying the sample type. |
General Data Type | TEXT |
Unit of Measure | |
Case Restriction | |
Display Example | |
Format Mask | |
Null Value | |
Null Value Meaning | |
Allowed Values | As provided |
Default Value | |
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Validation Rules |
Attribute Name | OA |
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Seq. Order | 7 |
Data Storage Type | TEXT |
Max Length | |
Min Length | |
Required | No |
Primary Key | No |
Precision | |
Scale | |
Status | Active |
Description |
The concentration of okadaic acid measured in a sample. Units for values are micrograms per 100 grams of tissue. |
General Data Type | TEXT |
Unit of Measure | micrograms per 100 grams of tissue |
Case Restriction | |
Display Example | |
Format Mask | |
Null Value | |
Null Value Meaning | |
Allowed Values | less than the limit of detection to the measured value |
Default Value | |
Foreign Key Relations | |
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Validation Rules |
Attribute Name | DTX-1 |
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Seq. Order | 8 |
Data Storage Type | TEXT |
Max Length | |
Min Length | |
Required | No |
Primary Key | No |
Precision | |
Scale | |
Status | Active |
Description |
The concentration of dinophysis toxin 1 measured in a sample. Units for values are micrograms per 100 grams of tissue. |
General Data Type | TEXT |
Unit of Measure | micrograms per 100 grams of tissue |
Case Restriction | |
Display Example | |
Format Mask | |
Null Value | |
Null Value Meaning | |
Allowed Values | less than the limit of detection to the measured value |
Default Value | |
Foreign Key Relations | |
Derivation | |
Validation Rules |
Attribute Name | DTX-2 |
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Seq. Order | 9 |
Data Storage Type | TEXT |
Max Length | |
Min Length | |
Required | No |
Primary Key | No |
Precision | |
Scale | |
Status | Active |
Description |
The concentration of dinophysis toxin 2 measured in a sample. Units for values are micrograms per 100 grams of tissue. |
General Data Type | TEXT |
Unit of Measure | micrograms per 100 grams of tissue |
Case Restriction | |
Display Example | |
Format Mask | |
Null Value | |
Null Value Meaning | |
Allowed Values | less than the limit of detection to the measured value |
Default Value | |
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Validation Rules |
Attribute Name | AZA-1 |
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Seq. Order | 10 |
Data Storage Type | TEXT |
Max Length | |
Min Length | |
Required | No |
Primary Key | No |
Precision | |
Scale | |
Status | Active |
Description |
The concentration of azaspiracid 1 measured in a sample. Units for values are micrograms per 100 grams of tissue. |
General Data Type | TEXT |
Unit of Measure | micrograms per 100 grams of tissue |
Case Restriction | |
Display Example | |
Format Mask | |
Null Value | |
Null Value Meaning | |
Allowed Values | less than the limit of detection to the measured value |
Default Value | |
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Validation Rules |
Attribute Name | AZA-2 |
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Seq. Order | 11 |
Data Storage Type | TEXT |
Max Length | |
Min Length | |
Required | No |
Primary Key | No |
Precision | |
Scale | |
Status | Active |
Description |
The concentration of azaspiracid 2 measured in a sample. Units for values are micrograms per 100 grams of tissue. |
General Data Type | TEXT |
Unit of Measure | micrograms per 100 grams of tissue |
Case Restriction | |
Display Example | |
Format Mask | |
Null Value | |
Null Value Meaning | |
Allowed Values | less than the limit of detection to the measured value |
Default Value | |
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Validation Rules |
Attribute Name | AZA-3 |
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Seq. Order | 12 |
Data Storage Type | TEXT |
Max Length | |
Min Length | |
Required | No |
Primary Key | No |
Precision | |
Scale | |
Status | Active |
Description |
The concentration of azaspiracid 3 measured in a sample. Units for values are micrograms per 100 grams of tissue. |
General Data Type | TEXT |
Unit of Measure | micrograms per 100 grams of tissue |
Case Restriction | |
Display Example | |
Format Mask | |
Null Value | |
Null Value Meaning | |
Allowed Values | less than the limit of detection to the measured value |
Default Value | |
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Validation Rules |
Attribute Name | Total OA equiv. |
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Seq. Order | 13 |
Data Storage Type | TEXT |
Max Length | |
Min Length | |
Required | No |
Primary Key | No |
Precision | |
Scale | |
Status | Active |
Description |
The sum of Okadaic acid, Dinophysis toxin 1 and Dinophysis toxin 2 for a given sample after equivalency factors have been applied. Units for values are micrograms per 100 grams of tissue. |
General Data Type | TEXT |
Unit of Measure | micrograms per 100 grams of tissue |
Case Restriction | |
Display Example | |
Format Mask | |
Null Value | |
Null Value Meaning | |
Allowed Values | less than the limit of detection to the measured value |
Default Value | |
Foreign Key Relations | |
Derivation | |
Validation Rules |
Attribute Name | PP2A |
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Seq. Order | 14 |
Data Storage Type | TEXT |
Max Length | |
Min Length | |
Required | No |
Primary Key | No |
Precision | |
Scale | |
Status | Active |
Description |
Result of the protein phosphatase 2A screening assay. Units for values are micrograms per 100 grams of tissue. |
General Data Type | TEXT |
Unit of Measure | micrograms per 100 grams of tissue |
Case Restriction | |
Display Example | |
Format Mask | |
Null Value | |
Null Value Meaning | |
Allowed Values | less than the limit of detection to the measured value |
Default Value | |
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Validation Rules |
Attribute Name | Shellfish Analysis Notes |
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Seq. Order | 15 |
Data Storage Type | TEXT |
Max Length | |
Min Length | |
Required | No |
Primary Key | No |
Precision | |
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Status | Active |
Description |
Notes regarding the analyses of specific shellfish samples. |
General Data Type | TEXT |
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Allowed Values | As provided |
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Child Items
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Related Items
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Catalog Details
Catalog Item ID | 54713 |
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Metadata Record Created By | Jeffrey W Cowen |
Metadata Record Created | 2018-11-08 11:33+0000 |
Metadata Record Last Modified By | SysAdmin InPortAdmin |
» Metadata Record Last Modified | 2022-08-09 17:11+0000 |
Metadata Record Published | 2018-11-08 |
Owner Org | NWFSC |
Metadata Publication Status | Published Externally |
Do Not Publish? | N |
Metadata Workflow State | Published / External |
Metadata Last Review Date | 2018-11-08 |
Metadata Review Frequency | 1 Year |
Metadata Next Review Date | 2019-11-08 |
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